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Ramachandran Azhakar, Herbert W. Roesky, Julian J. Holstein and Birger Dittrich Reaction of the Silylene PhC(NtBu)2SitBu with 4,4′-Bis(dimethylamino)thiobenzophenone and Treatment of the Silylene PhC(NtBu)2SiC(SiMe3)3 with 3,5-Di-tert-butyl-o-benzoquinone European Journal of Inorganic Chemistry 2013

Article first published online: 2 APR 2013 | DOI: 10.1002/ejic.201300085

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The reaction of LSitBu [L = PhC(NtBu)2] (1) with 4,4′-bis(dimethylamino)thiobenzophenone resulted in the [1+2]-cycloaddition product silathiacyclopropane 3, bearing a three-membered SiCS ring. The reaction of LSiC(SiMe3)3 (2) with 3,5-di-tert-butyl-o-benzoquinone leads to the [1+4]-cycloaddition product 4.

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