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Fumio Akagi, Shoui Suzuki, Yutaka Ishida, Tsubasa Hatanaka, Tsukasa Matsuo and Hiroyuki Kawaguchi Reactions of a Niobium Nitride Complex Prepared from Dinitrogen: Synthesis of Imide and Ureate Complexes and Ammonia Formation European Journal of Inorganic Chemistry 2013

Article first published online: 10 MAY 2013 | DOI: 10.1002/ejic.201300172

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The niobium nitride complex prepared from N2 was protonated to generate NH3, while the reaction with methyl iodide gave the methyl imide complex. Exposure of the imide complex to CO2 gave the ureate complex along with the oxo-bridged dinuclear complex.

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