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Thomas W. Myers, Gereon M. Yee and Louise A. Berben Redox-Induced Carbon–Carbon Bond Formation by Using Noninnocent Ligands European Journal of Inorganic Chemistry 2013

Article first published online: 22 MAY 2013 | DOI: 10.1002/ejic.201300192

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Oxidation of (IP)2Al(CH3) (IP = iminopyridine) with TrBPh4 (Tr = trityl) affords the C–C-coupled kinetic product [(IP)(Tr-IP)Al(CH3)][BPh4] in which the trityl radical and the IP radical have undergone C–C bond formation. Oxidation of (IP)2Al(CH3) with TrBArF24 affords the thermodynamic product [(IP)(IP)Al(CH3)][BarF24] {BArF24 = tetrakis[(3,5-trifluoromethyl)phenyl]borate}.

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