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Melanie Helms, Zhijie Lin, Lei Gong, Klaus Harms and Eric Meggers Method for the Preparation of Nonracemic Bis-Cyclometalated Iridium(III) Complexes European Journal of Inorganic Chemistry 2013

Version of Record online: 5 JUN 2013 | DOI: 10.1002/ejic.201300411

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By utilizing chiral auxiliaries, a practical strategy for the generation of enantiomerically pure bis-cyclometalated IrIII complexes was developed. The method relies on the synthesis and subsequent chromatographic separation of diastereomeric complexes followed by substitution of the auxiliaries with polypyridyl ligands with complete retention of configuration.

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