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Justus Tönnemann, Julie Risse, Zacharias Grote, Rosario Scopelliti and Kay Severin Efficient and Rapid Synthesis of Chlorido-Bridged Half-Sandwich Complexes of Ruthenium, Rhodium, and Iridium by Microwave Heating European Journal of Inorganic Chemistry 2013

Version of Record online: 5 JUL 2013 | DOI: 10.1002/ejic.201300600

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The important organometallic starting materials [(p-cymene)RuCl2]2 and [(cyclopentadienyl)MCl2]2 (M = Ru, Rh, Ir) can be obtained by microwave heating. This methodology shortens their synthesis times from several hours to a few minutes.

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