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Heiko Bauer, Daniel Weismann, Gotthelf Wolmershäuser, Yu Sun and Helmut Sitzmann Iron-Mediated Coupling of Two Ethyl Anions to Form a 2-Butyne Ligand European Journal of Inorganic Chemistry 2014

Version of Record online: 3 JUN 2014 | DOI: 10.1002/ejic.201402143

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With ethylmagnesium bromide, the high-spin iron(II) aryl complex [(C5HiPr4)Fe(C6H3-2,6-iPr2)] or the half-sandwich complex [(C5HiPr4)Fe(μ-Br)]2 forms the dinuclear complex [{(C5HiPr4)Fe}2(μ,η22-C2Me2)], a rare example of a metallatetrahedrane with a metal–metal triple bond.

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