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Ke Zhang, Xiao-Long Qiu, Yangen Huang and Feng-Ling Qing An Improved Copper-Mediated Oxidative Trifluoromethylation of Terminal Alkynes European Journal of Organic Chemistry 2012

Version of Record online: 29 NOV 2011 | DOI: 10.1002/ejoc.201101550

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Improved method for the efficient copper-mediated trifluoromethylation of terminal alkynes has been developed. This protocol highlights the convenient access to a variety of aryl-substituted trifluoromethylated alkynes by oxidative trifluoromethylation with two equivalents of TMSCF3 at room temperature.

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