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F. Pointurier and O. Marie Use of micro-Raman spectrometry coupled with scanning electron microscopy to determine the chemical form of uranium compounds in micrometer-size particles Journal of Raman Spectroscopy 44

Article first published online: 16 OCT 2013 | DOI: 10.1002/jrs.4392

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Micro-Raman spectroscopy coupled with scanning electron microscopy has been used for the first time to analyze micrometer-size particles of various uranium oxides [UO2, U3O8, UO3,and UO4 · 4(H2O)] deposited on carbon disks. Despite a loss of signal-to-noise ratio of an order of magnitude with regard to the stand-alone micro-Raman spectroscopy, all uranium oxides are successfully identified in particles by in-scanning electron microscopy Raman analysis. Moreover, particles as small as 1 µm can be analyzed.

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