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Artur Mardyukov and Armido Studer Preparation of Photoactive Polymers and Postmodification via Nitroxide Trapping Under UV Irradiation Macromolecular Rapid Communications 34

Version of Record online: 26 OCT 2012 | DOI: 10.1002/marc.201200595

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Nitroxide-mediated polymerization (NMP) and photoclick chemistry for the preparation of functionalized polymers are presented. A photoactive monomer is readily prepared on a large scale and is polymerized in a controlled manner by NMP to give polymer A. Photoirradiation provides via Norrish-type 1 cleavage the corresponding polymeric acyl radicals, which are trapped with a functionalized nitroxide to give the corresponding polymeric acylalkoxyamine B in high yield.

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