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Tsuguto Imaeda, Tamotsu Hashimoto, Satoshi Irie, Michio Urushisaki and Toshikazu Sakaguchi Synthesis of ABA-triblock and star-diblock copolymers with poly(2-adamantyl vinyl ether) and poly(n-butyl vinyl ether) segments: New thermoplastic elastomers composed solely of poly(vinyl ether) backbones Journal of Polymer Science Part A: Polymer Chemistry 51

Version of Record online: 29 JAN 2013 | DOI: 10.1002/pola.26561

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ABA-type triblock copolymers and AB-type star-shaped diblock copolymers with poly(2-adamantyl vinyl ether) [poly(2-AdVE)] hard outer segments and poly(n-butyl vinyl ether) [poly(NBVE)] soft inner segments were synthesized by sequential living cationic copolymerization. Although they are totally composed of poly(vinyl ether) backbones and hydrocarbon side chains, the two polymer segments were segregated into a microphase-separated structure to form thermoplastic elastomers with good mechanical and thermal properties and wide service temperatures.

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