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Maryluz Moreno, Gerard Lligadas, Juan C. Ronda, Marina Galià and Virginia Cádiz Flame retardant high oleic sunflower oil-based thermosetting resins through aza- and phospha-michael additions Journal of Polymer Science Part A: Polymer Chemistry 51

Article first published online: 6 FEB 2013 | DOI: 10.1002/pola.26562

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New flame retardant phosphorus-containing thermosetting resins have been prepared by phospha-Michael addition of a difunctional secondary phosphine oxide, the 1,3-bis(phenylphosphino)propane dioxide, and aza-Michael addition of 4,4′-diaminodiphenylmethane. Different materials with 0–4.2% of P were obtained starting from a high oleic sunflower oil enone derivative. The kinetics of the phospha and aza-Michael additions under various conditions was investigated using model compounds and the thermal stability and flame retardant properties of the final materials were evaluated by TGA and LOI measurements.

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