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Pinar Sinem Omurtag, Ufuk Saim Gunay, Aydan Dag, Hakan Durmaz, Gurkan Hizal and Umit Tunca Diels-alder click reaction for the preparation of polycarbonate block copolymers Journal of Polymer Science Part A: Polymer Chemistry 51

Article first published online: 19 FEB 2013 | DOI: 10.1002/pola.26608

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Well-defined α-furan protected maleimide-terminated poly(ethylene glycol) (PEG11-MI or PEG37-MI), poly(methyl methacrylate) (PMMA26-MI), and poly(ε-caprolactone) (PCL27-MI) were clicked with a PC-anthracene at reflux temperature of toluene to yield their corresponding PC-based block copolymers (PC-b-PEG, PC-b-PMMA, and PC-b-PCL). The homopolymer precursors and their corresponding block copolymers were characterized by using the GPC, NMR, and UV analysis.

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