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Dorota Koziej, Marta D. Rossell, Bettina Ludi, Andreas Hintennach, Petr Novák, Jan-Dierk Grunwaldt and Markus Niederberger Interplay Between Size and Crystal Structure of Molybdenum Dioxide Nanoparticles—Synthesis, Growth Mechanism, and Electrochemical Performance Small 7

Article first published online: 20 DEC 2010 | DOI: 10.1002/smll.201001606

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The rapid reduction of MoO2Cl2 precursor triggers the nucleation of 2 nm MoO2 nanospheres with a hexagonal crystal structure. An increase in particle size induces a crystal phase transition from hexagonal to monoclinic. The transformation from spheres into rods emerges as a complex process driven by oriented attachment.

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